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Method 5035A: Closed-system Purge-and-trap and Extraction for Volatile Organics in Soil and Waste Samples Published 2002
US EPA has updated its guidance to reflect the latest evaluation of currently available data and technologies for VOC sample handling and preservation procedures for solid samples. The procedures are designed to minimize VOC losses through the two most common mechanisms, volatilization and biodegradation. This guidance appears in SW-846 Method 5035A, which includes a 30-page appendix of detailed explanatory material.
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